EQUIPMENT & SUPPLIES: Samplers--P-61 and P-63 Point-Integrating Sediment Samplers In Reply Refer To: November 19, 1979 EGS-Mail Stop 412 QUALITY OF WATER BRANCH TECHNICAL MEMORANDUM NO. 80.03 Subject: EQUIPMENT & SUPPLIES: Samplers--P-61 and P-63 Point- Integrating Sediment Samplers The purpose of this Memorandum is to remind those people who use the P-61 and P-63 point-integrating samplers of one of the most common causes of malfunction of these samplers. If water gets into the head cavity, corrosive damage to the plug and solenoid assembly will cause the valve to stick and become inoperable if proper maintenance procedures are not taken. The valve which controls the nozzle and air openings is electrically controlled, and has two positions (see Fig. 2). In the power-off position the valve is in the pressure-equalizing position; the nozzle is closed, and air flows only from the compression chamber into the head cavity and from the head cavity into the bottle. This equalizes the pressure in the bottle with the hydrostatic pressure as the sampler is lowered through the water. In the power-on position the valve is in the sampling position; the nozzle is open, and the air flows only from the bottle into the head cavity and out through the air-exhaust opening. Water can get into the head cavity under the following conditions if: (References are to the enclosed drawings and parts list) l) no nozzle is in place. Water will rapidly fill the head cavity if a nozzle has not been properly installed. 2) the nozzle gasket is missing. Water will enter between the nozzle and nozzle nut. 3) the sampler is submerged without a sample container in the sampler. If the sampler is submerged without a container, water can enter the head when the valve is in the power-off position. In this position water can enter through the air-exhaust opening (Section B-B). Solution--never submerge a sampler without a bottle properly sealed in place. 4) the sample container is filled to the maximum recommended volume and the sampler is allowed to tilt forward more than about 10 degrees after the valve has closed (power-off position). Some water can run back through the air exhaust opening into the head (Section B-B). If the sample container is overfilled water will definitely enter the head cavity when the valve is closed (power off). Solution--do not overfill the sample container. Try to keep the sampler from tilting head down when retrieving and removing the sample container. 5) the nozzle is not tightened into the valve body and the nozzle nut is not tightened against the nozzle gasket (O-ring). The nozzle (part P61-11) must be hand-tightened into the valve body, then the nozzle gasket (P61-13) must be compressed by tightening the nozzle nut (P6l-l2) to prevent water from entering the head cavity around the nozzle. Solution--Loosen the nozzle nut before inserting and tightening the nozzle, and then use an adjustable wrench to tighten the nozzle nut gently against the O-ring. 6) the air-line gasket is worn or missing. The air-line gasket (P61-29) is seated into the sampler head. When the head is closed the gasket is pressed against the air-line opening in the body, thus completing the air line from the compression chamber to the head cavity and sealing it against leakage. If this gasket becomes worn or damaged (or is missing), water can enter the head cavity. Solution--The seal should be checked frequently by placing a paper strip against the gasket and closing the head. If the paper strip can be easily withdrawn, the gasket should be replaced before submerging the sampler. 7) rinse water is poured onto the gasket and nozzle area of the sampler head when the valve is in the power-off position. When these samplers are used to collect samples for chemical analysis, that part of the head which is in contact with the sample container is supposed to be rinsed with native water at the sampling site. If this is done while the sampler head is hanging open with the valve in the power-off position (Section B-B), some of the water that is poured onto the gasket and nozzle area can go directly into the head cavity through the air-exhaust opening. Solution--To rinse that part of the head and gasket which is in contact with the sample container, l) place a proper container in the sampler, 2) close the head, 3) submerge the sampler in the stream to be sampled, 4) open the valve (power on), S) leave the valve open long enough to fill the container about half full, 6) raise the sampler to the point where the tail fin can be grabbed, 7) open the valve (power on) and tilt the sampler up and down to rinse the contact area. Some water will be forced back through the nozzle, but will not get into the head cavity as long as the power is on. Discard the remainder and begin sampling. It would appear that it is almost impossible to use these samplers without allowing some water to get into the head cavity. It definitely is difficult to prevent leakage; however, if care is taken most problems associated with leakage can be minimized. If the operator removes the nozzle and the nozzle nut after sampling and opens the head while the sampler is in the suspended position, excess water in the head will immediately drain through the threaded nozzle-nut opening. Since air is free to flow through the pressure-equalization hole near the hinge, if the sampler is stored with the head open and the nozzle and nozzle nut removed, the head cavity should dry within a few hours. A tire pump or other compressed air source could be used to accelerate the drying process. Other points to remember are: 1, Disassemble the head and clean all parts frequently. If the sampler is only infrequently used it should be cleaned following each trip. 2. Be sure that the power supply is fully charged. 3. Make sure that there is direct contact between the hanger bar and the Type B connector. Do not use a Type B connector with a nylon bushing (See WRD Equipment Catalog, stock number 434003), but do use the Type B connector with brass bushing (stock number 434002). 4. Do not use damaged nozzles. 5. The head gasket is seldom a source of leaks. Do not use gasket cement. If the head gasket must be replaced, order a replacement from the Sedimentation Project. Use of a gasket having improper thickness will cause misalignment between the nozzle nut and valve body. 6. Never submerge a sampler beyond its rated depth (180 feet with pint container or 120 feet with quart container). A copy of the Instructions for US P-61-Al Suspended Sediment Sampler is attached. All operators using point-integrating samplers should be entirely familiar with these instructions. R. J. Pickering Enclosure WRD Distribution: A, FO FEDERAL INTER-AGENCY SEDIMENTATION PROJECT St Anthony Falls Hydraulic Laboratory Hennepin Island & Third Ave S E. Minneapolis, Minnesota 55414 INSTRUCTIONS FOR US P-61-Al SUSPENDED SEDIMENT SAMPLER These instructions describe the sampler, present detailed maintenance procedures, and outline general operating techniques They are not intended as a comprehensive field guide For details that pertain to sampling theory and sample analysis, refer to Report No 14(1), Techniques of Water-Resources Investigations of the U S. Geological Survey(2), and the ASCE Sedimentation Engineering Manual(3). Purpose The US P-61-Al was designed to collect special samples required to determine the suspended-sediment discharge of a river or stream. The sampler may be used to collect either depth-integrated samples or point-integrated samples. Before shipment each sampler is checked and, if necessary, adjusted to sample at, or very near, stream velocity. To maintain the adjustment and thereby insure samples of high quality, operators are urged to review and follow these instructions. Physical Characteristics The sampler is cast of bronze, weighs 105 pounds, has an overall length of 28 inches and an overall height slightly less than 13 inches (fig 1). It will hold either a quart (Owens ~ Illinois #6762) or pint (round glass milk bottle) sample container The sampler consists of two major parts; the head and the body. The head supports both the sampling nozzle and the electrically- operated, two-position rotary valve Also, it contains several passageways that convey air and water The body supports the sample container, and the tail vanes which align the nozzle with the approaching stream flow The body has a hollow interior which serves as a compression chamber that forces air into both the head cavity and the sample container. A latch and hinge hold the head and body together. The head pivots on the hinge and swings away from the mouth of the sample container Valve Mechanism The valve serves two purposes: it starts and stops both liquid flow into the sample container and air flow to and from the container. The porting diagram for the valve is shown in fig 2 With no electrical power applied, the valve is in the pressure equalizing position As the sampler is lowered through the water, hydrostatic pressure forces-water through the holes in the belly of the sampler and then into the compression chamber Air inside the chamber flows through the tube that leads to the head cavity At the head-body junction, the air flows through the air line gasket (part 29, fig 1) Air in the head-cavity flows through the valve plug (fig 2, section B-B, pressure equalizing position) and into the sample container The air flow balances the pressure inside the sample bottle with that near the nozzle. ~hen power is applied, the solenoid turns the valve into the sampling position, fig 2. The connection to the compression chamber closes and the passage leading from the nozzle to the sample container opens. Without surging, the sample flows into the sample container Leading from the sample container to the ambient flow, another passage steadily expels air displaced by the sample Sampling terminates when power is removed and the valve plug returns to the equalizing position Power Supply To support the sampler and to transmit power, the sampler must be suspended on a sheathed single-conductor cable To minimize drag, the cable should have a diameter of 1/8" or smaller. To minimize power supply voltage, the resistance should not exceed 100 ohms per 1000 feet An Ellsworth cable is commonly used and may be purchased from the U S Geological Survey, Shipping and Receiving Section, Mail Stop 231, Reston, Virginia 22092. Connect the sheath, exterior load-bearing strands, to a special clamp and pin the clamp to the top end of the hangar bar. Connect the insulated conductor, located in the center of the cable, to the insulated wire on the left side of the head. This completes connections at the sampler end of the cable On the reel end, secure the cable to the reel then connect the center conductor ~o the slip-ring. When power is applied at the reel, current will flow from the supply, through the center conductor and then through the solenoid Current will return through the sampler body, the hangar bar, the cable sheath, and the reel frame The power supply must be direct-current which, at remote sites, is most conveniently obtained from dry or wet cell batteries The supply voltage is set by the required current and the total resistance in the cable and solenoid. For a 100 foot cable with a resistance of 100 ohms/1000 feet, the cable resistance will be 10 ohms. The rotary solenoid has a resistance of 24 ohms and will require one ampere to rotate the valve With this cable, the voltage must be no less than 36 volts To provide for a margin of reliability and for battery discharge, a 48 volt d c supply is recommended. Eight 6-volt "hot shot" batteries or from eight to ten 6-volt lantern batteries can be used Other batteries such as wet cells can be used, but any battery selected must have capacity sufficient to sustain the required voltage while delivering a current of one ampere. A special capactive-discharge supply (BP- 76) may be purchased from the Sedimentation Project. Compared to batteries, the unit is lighter and smaller but is more expensive. Accessories For field sampling with the P-61, a cable, power supply, switch, crane, reel, cable connector, hangar bar, and hangar bar pin are required. Most of these items can be obtained from the Geological Survey at Reston, Virginia A standard threaded hangar bar pin is recommended but a plain 3/8" x 3" diameter steel pin may be substituted. If a plain pin is used the hangar bar must have a smooth hole rather than a threaded hole. The set screw, (P61-25, fig. 1) must be installed to retain the pin. With a battery supply a single-pole single-throw toggle switch will be required This type of switch is available at local hardware or electronic stores. Six to ten feet of 14 AWG stranded, insulated wire and two clips will be needed to connect the batteries to the reel. The BP- 76 includes a switch and wire. Operation Fasten one end of the cable to the reel and connect the center conductor to the reel slip-ring. ~eel the cable onto the drum, mount the reel on the crane, then thread the cable over the crane sheaves. Clamp the other end of the cable into the cable- connector, then suspend the sampler on the hangar bar. Connect the center conductor to the sampler lead wire. On the power supply connect one wire to the reel slip-ring and connect the other wire to the frame of the crane or reel. The P-61 solenoid is not sensitive to direction of current so connections can be made without regard for polarity. Check for rotation of the valve plug by operating the switch several times while sighting through the nozzle. If the sampler has been in storage, water-formed deposits may cause the valve plug to seize in the valve plug body. If the valve will not turn, connect the power supply directly to the sampler leat-wire, apply power, and strike the side of the sampler head with a rubber or wood mallet. Never strike the nozzle. If a few sharp blows will not free the valve, refer to the Maintenance Section When the valve is operating properly, insert a sample bottle then close the head slowly. Guide the lip of the bottle so that it centers and seals against the face of the bottle gasket. Insert the aluminum adapter into the sample-container cavity if pint bottles are to be used Lower the sampler to the desired depth, then close the switch for the desired sampling interval. Open the switch, hoist the sampler, ant remove the sample bottle Optimum sampling intervals vary with stream velocity and container size, so some experimentation will be necessary The interval must be chosen so that the container is approximately 2/3 full Samples that are overfilled must be discarded and the process repeated with a shorter interval To be valid, a sample must enter the container only through the nozzle with a pint container the bronze P-61-Al sampler will function properly to a depth of 180 feet but with a quart container, the depth is only 120 feet At greater depths,water instead of air, will flow from the compression chamber and enter the sample container To collect a point-integrated sample, support the P-61 at a fixed depth during the entire sampling interval To collect a depth- integrated sample first open the valve then depending upon depth and velocity, either raise or lower the sampler at a uniform rate. If the stream is less than 18 feet deep and the velocity is moderate, close the switch to open the valve then lower the sampler at a uniform rate from the water surface to the bottom of the stream When the sampler touches bottom, instantly reverse reel rotation and,at a uniform rate, hoist the sampler through the flow. Switch the power off only after the sampler emerges from the stream If the stream is between 18 and 30 feet deep, or has a high velocity, the sampler may be used to depth-integrate in one direction, from the bottom of the stream to the surface With power off, lower the sampler to the stream bed. Apply power then, at the same instant, start hoisting at a uniform rate Switch power off when the nozzle breaks through the surface Deep, fast streams may be depth-integrated in sections At each sampling station, divide the vertical into several segments, then depth-integrate each segment individually When depth-integrating, never lower or hoist the sampler at a rate that exceeds 0 4 of the mean stream velocity For shallow streams transit rates are less Report No 14, p. 45 shows rate limits imposed by each of several factors Refer to the diagram for the 3/16" nozzle With the quart container, maximum rates as limited by air compression must be reduced to 1/2 of those shown in Report No 14(4). When handling a P-61 filled with a sample, never allow the nose to tilt down more than ten degrees. A portion of the sample may escape through the tube leading to the compression chamber Those unfamiliar with sampling theory or program objectives, must consult with the hydrologist to clarify details such as the number and the location of sampling stations within a particular cross section Maintenance If the valve plug fails to turn, disassemble the head. Remove the nozzle, then remove the hinge pin to free the head from the body To free the head the catch may be left in place, however, if the catch mechanism is to be disassembled take precaution to restrain the spring under the catch With the head free of the body, remove the six cap-screws that hold the head-base to the head-cover Separate the two parts and avoid damage to the gasket To disassemble the valve mechanism, first remove the screw in the end of the valve plug, then remove the washer, spring, and spring boss Note the shape of the valve arm and its orientation Punch marks on the valve plug and valve arm show their correct alignment The solenoid must be removed to free the plug from the valve body On the band that holds the solenoid, loosen the set-screw and remove the exposed screw that anchors the band. Note the orientation of the solenoid leads, then slide the solenoid free of the band Now slide the valve plug out of the valve body Use fine steel wool or fine sandpaper to clean and polish the plug and the inside of the valve body Household cleansers should not be used because the abrasive may become imbedded in the brass valve body and cause the plug to bind To check the solenoid, apply voltage directly to the solenoid lead wires. When power is applied, the solenoid should rotate 45! then, when power is removed, the solenoid spring should return the armature to its rest position If the solenoid fails to turn, corrosion may have damaged the winding or ball-race Replace the complete solenoid. To reassemble, reverse the above procedure The clock-type spring should be wound approximately 1/2 revolution and mounted so that movement of the valve to the sampling position tightens the spring. After all parts are assembled energize the solenoid. The valve arm should seat tightly against the stop and the valve plug sampling-intake hole should align with the corresponding hole through the valve body. If necessary, adjust the solenoid so that it does not bind against the valve wheel Clean the surface of the head gasket, position the head cover, then insert the six cap screws. Seat the screws firmly but do not tighten Face the screw heads and rotate the head so that the catch is at the 12 o'clock position. At the two o'clock position, label the screw number 1 In a clockwise direction label each screw then tighten in the sequence 1-4-6-3-5-2 Repeat the tightening sequence two or three times, each time increase the torque. Final torque should be 100- 125 pound inches. The exact torque is not critical but all screws should be tightened as nearly equal as "feel" permits Corrosive damage to the plug and solenoid assembly is caused by water that collects in the head cavity Even a small quantity will cause problems if the sampler is stored before removing the water When sampling is complete, remove the head base Drain and, with a cloth, dry ~he interior of the head cover then let the assembly air-dry before reinstalling the base. Slow leaks around the valve plug are unavoidable because the plug must be loose enough to rotate freely Parts that are missing or defective will cause serious leaks. A missing or defective nozzle gasket (o-ring) will allow water to leak into the head A worn or missing air-line gasket will allow water to enter the head and will interfere with the compression process. To seal, the air-line gasket must be pliable To check for seal, open the head, place a paper strip against the body where the gasket makes contact, then close the head If the paper is loose or can be withdrawn easily, replace the gasket. Contrary to expectations, the head gasket is seldom a source of leaks. Do not use gasket cement If the head gasket must be replaced, order a replacement from the project. In emergencies, gaskets may be cut locally, but be sure to use gasket stock of the same thickness as the original. Improper gasket thickness will cause misalignment between the nozzle ~and valve body. Even with good seals, improper operation can cause damage. If the sampler is submerged to depths beyond its rating or if the sampler is submerged without a proper sample container, the compression chamber will fill and water will enter the head through the compression line. A nozzle that is bent or burred around the ends will contribute to sampling errors and must be replaced. Replacement parts may be ordered from the Federal Inter-Agency Sedimentation Project. Also, samplers that require maintenance or recalibration may be shipped to the project. (l) Inter-Agency Committee on Water Resources, "Determination of fluvial sediment discharge," Rept 14, A study of methods used in measurement and analysis of sediment loads in streams; Subcommittee on Sedimentation, Minneapolis, Minnesota, 1963. (2) Guy, H. P.; Laboratory theory and methods for sediment analysis, Techniques of water-resources investigations of the U. S. Geological Survey, bk 5, ch Cl, 1969. (3) American Society of Civil Engineers, "Sedimentation Engineering," by Task Committee, V. A Vanoni, ed , ASCE, New York, N. Y., 1975. (4) Inter-Agency Committee on Water Resources, "The design of improved types of suspended sediment samplers," Rept. 6, A study of methods used in measurement and analysis of sediment loads in streams; Subcommittee on Sedimentation, Minneapolis, Minnesota, 1952, p 22-34