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SEE FLIGHT EXPERIMENTS / NEUTRAL EXTERNAL CONTAMINATION

Quick Look Report:
DTO-829 (STS-74) Plume Impingement Contamination

Dr. Steve Koontz

DTO-829 Objectives and Background
DTO-829 Flight Procedures and Mission Environments
DTO-829 Results and Discussion
Conclusions
Acknowledgments


DTO-829 Objectives and Background

The objective of Detailed Test Objective 829 (DTO-829) was to provide QCM measurements both transient and persistent surface contamination produced by: 1) Shuttle Primary Reaction Control System (PRCS) engines, 2) Russian 13 kg attitude control and reboost thrusters on Mir, and 3) the Shuttle environment during nominal operations. The last measurement, (3), provides additional sensor background data in the on-orbit Shuttle cargo bay environment to support data analysis. The DTO-829 data objectives were achieved during STS-74. Final data analysis will be completed following post-flight sensor thermal calibration at QCM Research, the sensor vendor. QCM research is preparing a cost estimate for the thermal calibration at this time and final data analysis and reporting is expected by September 30, 1996. The post flight thermal calibration is needed because QCM sensors are very sensitive to the thermal environment. Sensor output changes as a result of varying radiant heat transfer environments (deep space viewing, sun viewing and earth viewing), even when thermostated. Different sensor-output thermal effects are obtained for different external and internal heating functions so that the post flight thermal calibration had to be designed around the as- flown thermal environments of STS-74 which could only be determined post-flight. Preliminary results using pre-flight sensor thermal correction functions are, however, reported below.

The DTO-829 measurement objective was determined by the need to assess the impact of hypergolic engine plume impingement contamination on the functional life of sensitive International Space Station (ISS) surfaces. These assessments are important cost drivers for the ISS program because the outcome of the assessments are used to: 1) predict functional life, 2) set hardware replacement schedules, and 3) choose proximity operations scenarios. Assessments produced during the Space Station Freedom program showed that the then current engine plume contamination estimates, derived from ground- based, small-engine laboratory data (laboratory vacuum systems have vacuum pumping speeds that are only a small fraction of the equivalent vacuum pumping speed of the space environment) or Apollo-Skylab data, predicted significant degradation of both photovoltaic panels, and thermal control surfaces. Particle impact damage to the Space- Shuttle-Orbiter body flap tiles caused by vernier engine plume impingement seemed to qualitatively confirm the assumptions about engine plume contamination used in the early SSF assessments while raising new issues in the area of surface erosion by particle impact. Program cost growth resulting from limited subsystem life and/or operational fixes were possibilities indicated by these early assessments.

Only the relatively large PRCS engines fire at space station during the terminal phase of proximity operations. The CONTAM hypergolic engine simulation software package maintained by the Chemical Propulsion Information Agency at Johns Hopkins University predicts that Shuttle PRCS engines burn propellant more efficiently and produce far fewer damaging particles than either Shuttle vernier engines or the small laboratory scale engines used to establish the basis for the early SSF program engine plume contamination assessments. CONTAM predictions were also more consistent with Johnson Space Center space flight experience, for example with the Induced Environment Contamination Monitor (IECM) contamination monitor subjected to PRCS engine plumes during STS-2 to STS-5, showed no visible evidence of plume exposure. In addition the Soviet Program has reported some anecdotal information on the subject of hypergolic engine plume contamination or surface damage, though except for view port transparency reduction, no important system impacts were established. The Soviet and later Russian experience is important in light of the fact that the Russian 13 kg thrusters are similar to the Shuttle verniers in overall size and performance.

Space flight experience and CONTAM predictions both suggested that the basis for the SSF engine plume effects assessment was far too conservative and that significant cost avoidance was possible if a more realistic assessment basis could be established. Alternately, real proof of the validity of the earlier conservative basis for the assessment was needed to justify the implicit increase in program cost and complexity. The plume sticking fraction, i.e. the mass fraction of the total plume gas flow which sticks permanently on a sensitive surface is the most important factor in the ISS contamination effects and functional life assessments. The plume sticking fraction, expressed as a percentage of engine plume mass flux, was estimated at 1.0 percent, on the basis of the data sources described in the previous paragraph, during early SSF assessments.

During STS-52, direct QCM measurements of PRCS engine plume contamination with the Shuttle Plume Impingement Experiment (SPIE) revealed no detectable persistent or transient contamination with a QCM sensor temperature range of 305 to 330 degrees Kelvin. SPIE QCM data combined with post flight chemical analysis of SPIE hardware resulted in program acceptance of a new plume sticking fraction percentage of 0.02 percent, a conservative estimate based on sensor and analysis precision and accuracy limits only, in that no definite deposition was observed. The Shuttle Plume Impingement Flight Experiment (SPIFEX) payload which was subjected to numerous PRCS and vernier engine plume impingement events during STS-64. Post flight chemical analysis of SPIFEX witness coupons resulted in an even lower estimate of the persistent sticking fraction of 0.001 percent, the greater apparent sensitivity resulting from the very large number of engine plume impingement events compared to SPIE. DTO-829 was designed to verify, in a general way, the results of SPIE and SPIFEX on Shuttle PRCS engines while making a first set of measurements on the Russian 13 kg thrusters. By passively cooling the QCM sensors prior to the plume impingement events, more transient deposition should be observed. Atomic oxygen (AO) and solar ultraviolet (UV) were combined with plume impingement to determine if transient deposition can be fixed permanently by AO/UV in the low-Earth orbit (LEO) environment, a phenomena observed in ground based laboratory studies.

The experiment logic defining DTO-829 procedures and data analysis is somewhat different from that defining SPIFEX. The SPIFEX sticking fraction estimate was derived from post-flight analysis of witness coupons subjected to repeated engine plume impingement. The SPIFEX data is subject to some uncertainty resulting from prolonged exposure of the witness coupons to ambient atmosphere prior to analysis (some speculation concerning the possible evaporation of persistent plume contamination after exposure to humid air has been voiced from time to time). Therefore, DTO-829 was planned to provide measurements of engine plume contaminant deposition and re- evaporation phenomena in the space environment, with the best possible sensitivity given the limitations imposed by mission time line, sensor engine plume heating, and propellant utilization. Pre-flight planning calculations showed that the DTO-829 sensor set should be able to detect persistent sticking fractions greater than 0.003 percent of the net plume mass flow for the PRCS engines and greater than 0.01 percent for the Russian 13 kg thrusters.

DTO-829 Flight Procedures and Mission Environments.

DTO-829 was successfully carried out during STS-74. Two nominally identical Quartz Crystal Microbalance (QCM) sensors were mounted on the Shuttle remote manipulator end effector (RMS EE) and operated using a payload general services computer (PGSC, IBM Think Pad) interfaced to the sensor flight electronics unit (FEU). Both the computer and the FEU were mounted in the Shuttle aft flight deck area. The National Instrument Corporation's "LabVIEW for Windows" instrument control and data acquisition software package was used with the PGSC to provide a flexible and user friendly crew interface to DTO-829. Floppy disks containing the flight experiment data were provided to the DTO-829 Investigator less than two weeks after Shuttle landing.

DTO-829 consisted of three operational periods: 1) measurements of engine plume contamination produced by the Russian 13 kg thrusters, 2) a long term observation (about 16 hours) of the Shuttle cargo bay, and 3) measurements of Shuttle primary reaction control (PRCS) engine plume contamination. The Shuttle-Mir operations were completed at an altitude of 215 nmi (398 km) and the Shuttle-PRCS measurements were conducted at an altitude of 185 nmi (342 km). Atomic oxygen ram flux depends on both altitude and solar activity, measured as the 10.7 cm radio flux and the geomagnetic index Ap. The average value of the daily10.7 cm radio flux between Nov. 13 and Nov. 19, 1996 was 75plus minus1.2 and the average value of Ap was 4.14 plus minus 1.4 (Reported by NOAA, Boulder, Colorado). The atomic oxygen ram flux depends primarily on the magnitude of Ap and the 10.7 cm radio flux and the spacecraft orbital altitude. The approximate oxygen ram flux of 3 x 10 **13 O-atoms/cm**2sec. at 398 km altitude and 6 x 10 **13 O-atoms/cm**2sec. at 342 km (more accurate calculations of the atomic oxygen flux incident on the sensors during STS-74 are in progress).

The attached figures 1 and figure 2 show the Shuttle RMS configuration for each of the plume impingement measurements. Prior to both Mir and Shuttle engine contamination measurements the sensors were oriented to deep space to produce passive radiative cooling to below 300 K, though conflicting pointing requirements prevented cooling to below 280 K. The Shuttle-MIR stack attitude during the Mir jet measurements was defined as IO 5.1. The Shuttle attitude during the PRCS measurements -XLV, -YVV. For the Mir 13 kg thruster measurements the sensors were 40 feet away from the subject thruster and positioned on the engine plume axis, with the sensor-set normal directed at the thruster. For the Shuttle PRCS measurements (figure 2) the sensors were on plume axis, 34.7 feet away from the F3U PRCS engine. In this case the angle between the sensor normal and the engine plume was 35 degrees to accommodate the need for simultaneous exposure to the atomic oxygen ram flux and solar ultraviolet during the engine firings. The angle between the sensor normal and the sun vector was 9 degrees and the angle between the velocity vector and the sensor normal was 35 degrees.

Long term observations of the shuttle cargo bay involved parking the RMS above the cargo bay with the sensor-set normal pointed toward the center of the cargo bay (RMS EE coordinates were X=-575 inches, Y=+5.50 inches and Z=-740 inches in the Shuttle operations coordinate system). The sensors were not actively heated during this time so that frequency changes reflect passive thermal heating and cooling effects resulting from changes in the radiative thermal environment during each orbit.

DTO-829 Results and Discussion

Sensor frequency and temperature data for sensor B is shown in figure 3 (Mir jet firings), figure 4 (Shuttle cargo bay observation period), and figure 5 (Shuttle PRCS measurements). Mass deposition on the sensors produces an increase in the output frequency of the sensors, however various thermal effects also change sensor frequency. Throughout the mission sensor A produced more noise in the frequency data than sensor B so that the sensor A data is viewed as less reliable than sensor B data (sensors A and B showed qualitatively similar responses).

The calculation of engine plume sticking fraction estimates from QCM sensor frequency data requires an estimate of the total engine plume mass flux to the sensor during the experiment as well as the mass deposited on the sensor. Mass deposition is calculated from change in sensor output frequency, deltaf (with frequency output corrected for thermal effects), resulting form the mass deposition event, and then multiplying deltaf by the sensor mass-frequency calibration constant (equation 1).

(f2 (Hz) - f1 (Hz)) x 4.42 x 10-9 (g/cm**2 Hz) = G(g/cm**2 ), (1).

where

f2 = sensor frequency, corrected for thermal effects, after the mass deposit event, f1 = sensor frequency, corrected for thermal effects, before the mass deposit event, G = grams/cm**2 deposited on the sensor.

The 13 kg Mir engine and the Shuttle PRCS engine both produced an immediate contamination mass deposit as indicated by the increase in sensor output frequency coincident with the engine firing event. Using equation 1, the immediate mass deposit for each engine can be calculated.

Mir 13 kg engine initial deposit = 0.62 micrograms/cm**2

Shuttle PRCS engine initial deposit = 15.6 micrograms/cm**2

The initial deposit from both engine types sublimed or evaporated rapidly so that the sensor output frequency, corrected for thermal effects, was near the pre-mass deposit value by the end of the experiment period indicating that little or no persistent mass deposition had resulted from the engine firings. Because small differences in sensor output frequency are involved in the calculation of the amount of persistent mass deposit and the final post-flight sensor thermal re-calibration will not be completed for several months, the estimates of the persistent mass deposit given below are provisional. Nonetheless, little or no persistent mass deposit is indicated from either engine type and no important increase in the estimated mass deposit is anticipated.

Some comment on the thermal effects visible in the expanded scale data plots is appropriate. Abrupt step-function changes in frequency are associated with movement into and out of sunlight as is shown in figure 4, figure 6, and figure 7. The direct photothermal effect is well known in the industry and the instrument vendor verifies that the effect is of the correct order of magnitude in DTO-829 data set. In addition, sensor assembly temperature changes, measured by a thin-film resistance thermometer on the sensor crystal. Both effects are taken into account when calculating deltaf.

Mir 13 kg engine persistent deposit = 0.01 + 0.09 micrograms/cm**2

Shuttle PRCS engine persistent deposit = 0.1 + 0.09 micrograms/cm**2

A preliminary estimate of the engine plume persistent sticking fraction (the basis of the ISS contamination performance and functional life estimates as described above) can be made using simple rocket engine plume models to estimate the engine plume mass flow past the sensor location during the test. The PRCS engine plume model is used directly and the Mir 13 kg engines are modeled using a model of the Shuttle vernier engine plume, since the Russian 13 kg thruster is nearly identical to the Shuttle vernier in size, thrust and propellant mass flow rate (differences in propellant mass flow rate were taken into account). More detailed calculations using current ISS program baseline engine plume models are in progress, however, no important change in the conclusions are anticipated at this time because DTO-829 measurements were conducted on engine plume axes. The persistent sticking fraction is calculated by dividing the measured sensor mass deposition by the total engine plume mass flow delivered to the sensor location (calculated using the approximate plume models given in the Shuttle/Payload Contamination Evaluation Program MCR-81-509, NAS9-15826, Feb. 1981.).

Mir 13 kg engine persistent sticking fraction (percent) = 0.006 plus minus 0.05 percent

Shuttle PRCS engine persistent sticking fraction (percent) = 0.007 plus minus 0.006 percent

Conclusions

The sensitivity of any technique used to measure the sticking fraction of rocket engine plume gases in the LEO environment is ultimately limited by the sensor signal to noise ratio and the total mass flow of plume gases over the sensor. The results of DTO-829 confirm the SPIE results for Shuttle PRCS engines and extent the measurement to greater sensitivity as a result of the increased number of engine firings and the smaller separation between the sensor set and the F3U engine. In addition, cooling the sensors allowed for a greater transient contamination deposit which did not show detectable permanent fixation as a result of the combined effects of atomic oxygen and solar UV radiation. Finally, the first measurements, to which we have access, of contamination produced by the Russian 13 kg engines have been made and no persistent contamination has been detected which alleviates some program concerns about 13 kg engine plume degradation of the ATCS radiators on ISS. SPIE, SPIFEX, and DTO-829 together, provide the data needed to set the persistent plume sticking fraction for hypergolic engines of interest to the International Space Station Program at 0.001 percent of the net plume gas flow for contamination assessment and functional life predictions. The estimate of 0.001 percent is based on SPIFEX measurements and observations confirmed by the fact that DTO-829 measurements revealed no persistent contamination with a comparable though somewhat lower sensitivity. An accurate and realistic basis for performance assessments leads directly to significant program cost avoidance and reduced program risks.

Acknowledgments

Payload integration, payload development, flight planning and flight operations support were excellent throughout this DTO effort. EV/Gary Bourland did an excellent job with developing the LabVIEW Windows software application to DTO-829 despite the difficulties involved with the ongoing change from the Grid to the IBM Thinkpad PGSC platform. MT2/Vanessa Ellerbe developed the Integration Plan (IP) and Annexes that made the integration process proceed smoothly and efficiently despite the need to develop joint operations with the Russian Program during IP development. DF44/RSO/Alberto Magh Developed RMS procedures for both the Shuttle and Mir components of the mission. The Paylaod Officer, DO621/Tim Baum, and the Timeliner, DO451/Gail Schneider, were especially helpful in negotiating the joint operations agreement with the Russian Program, which ultimately agreed to commit 8 kg of valuable propellant and develop custom thruster firing software to support the DTO-829 measurements. OB/ETS/Buck Gay provided invaluable assistance in interfacing with the Russian Program. KSC support (Bob Peterson, Tom Kelley, and the RMS support team) was excellent and included a custom modification of an RMS EE thermal blanket to accommodate the DTO 829 QCM sensor set, though some misunderstandings developed in the area of PGSC support for the in vehicle test (IVT) (probably as a result of the PGSC platform change process).

Flight operations support was also excellent with controllers and back-room staff showing a detailed knowledge of the DTO-829 requirements and informing the PI of any deviations. OB/ETS/Carolynn Conley provided excellent support in the CSR during the mission. 


 

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