HFMRF Instrumentation

Varian INOVA 800

The Varian 800 is an INOVA based spectrometer and an Oxford 18.8 T magnet with a 63 mm room temperature bore. This system is capable of high resolution liquid and solid state NMR. There are 4 RF channels with waveform generators and pulsed field gradients. The wideline ADC's run at 5 MHz and the narrow ADC's have a maximum rate of 500 kHz. We currently have a 5 mm HCN probe with Z-gradient for liquids and a single tuned 5 mm MAS probe. Under construction are a 5 mm orthogonal powder probe optimized for low gamma nuclides, a 5 mm HX MAS probe (12 kHz spinning), and a 4 mm HXY MAS probe (25 kHz spinning).

Varian INOVA 750

The Varian 750 is an INOVA based spectrometer and an Oxford 17.6 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquids, solid state NMR and µ-imaging. There are 4 RF channels with waveform generators and pulsed field gradients. The narrow ADC's have a maximum rate of 500 kHz. We currently have two 5 mm HCN probes (Z-gradient), an 8 mm HCN probe (Z-gradient), a 5 mm HCP probe (Z-gradient), a 5 mm HX MAS probe (10 kHz spinning) and a µ-imaging probe.

Varian INOVA 600

The Varian 600 is an INOVA based spectrometer and an Oxford 14.1 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquid. There are 4 RF channels with waveform generators and pulsed field gradients. The narrow ADC's have a maximum rate of 500 kHz. We currently have a 5 mm HCN probe with Z-gradient and a 5 mm HX probe.

Varian Unity 600

The Varian 600 is an Unity based spectrometer and an Oxford 14.1 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquid. There are 3 RF channels with waveform generators and pulsed field gradients. The narrow ADC's have a maximum rate of 500 kHz. We currently have a 5 mm HCN probe with Z-gradient and a 5 mm HX probe.

Varian Unity+ 500

The Varian 500 is an Unity+ based spectrometer and an Oxford 11.7 T magnet with a 89 mm room temperature bore. This system is capable of solid state NMR, µ-imaging and small animal MRI. There are 3 RF channels with waveform generators. The wideline ADC's run at 5 MHz. We currently have a 5 mm orthogonal powder probe, 5 mm HXY MAS probe (15 kHz spinning), a 7 mm HX MAS probe (10 kHz spinning), an HX single crystal probe, a 1H CRAMPS probe, a micro-coil imaging probe, and a 40 mm imaging probe. Under construction are a combined µ-imaging and optical microscope probe and a static HX low temperature probe (2 - 300 K).

Varian/Chemagnetics Infinity 500

The Chemagnetics 500 is an Infinity based spectrometer and an Oxford 11.7 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquid and solid state NMR. There are 3 RF channels. We currently have a 5 mm HCN probe, a 10 mm HX probe, and a 5 mm HX MAS probe.

Varian Unity+ 500

The Varian 500 is an Unity+ based spectrometer and an Oxford 11.7 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquids NMR. There are 3 RF channels with waveform generators and pulsed field gradients. We currently have a 5 mm HCN probe with Z-gradient and a 10 mm HX probe.

Homebuilt/Tecmag 400

The homebuilt 400 spectrometer is based on homebuilt transmitter/receiver RF sections, a Tecmag pulse programmer and signal averager, and an Oxford 9.4 T magnet with a 89 mm room temperature bore. This system is capable of solid state NMR. There are 2 RF channels and 4 MHz ADC's. We currently have a 5 mm orthogonal powder probe, a 5 mm HX static low temperature probe (3.8 - 300 K), a 7 mm HX static low temperature probe (4.2 - 400 K), a 10 mm HX DAS probe.

Varian/Chemagnetics Infinity 300

The Chemagnetics 300 is an Infinity based spectrometer and an Oxford 7.04 T magnet with a 89 mm room temperature bore. This system is capable of high resolution liquid and solid state NMR. There are 3 RF channels. We currently have a 5 mm HX probe, a 10 mm HX probe, a 7.5 mm HX MAS probe, and a 5 mm orthogonal powder probe.

Varian Unity+ 300

The Varian 300 is an Unity+ based spectrometer and an Oxford 7.04 T magnet with a 89 mm room temperature bore. This system is capable of solid state NMR, µ-imaging and small animal MRI. There are 2 RF channels with wideline ADC's running at 5 MHz. We currently have a 7 mm HX MAS probe (10 kHz spinning), an HX single crystal probe, a 1H CRAMPS probe, a single tuned DOR probe, an HX 5mm low temperature MAS probe (35-300K, 12 kHz spinning), a 7 mm HX High temperature probe (-100 - 500°C, 7 kHz spinning), a microscopy probe and a 40 mm imaging probe.

Bruker Pulsed EPR/ENDOR/ELDOR Spectrometer

The EPR/ENDOR work focuses on the development and application of pulsed-2D methods for electronic structure and distance determinations in biological macromolecules and materials. The spectrometer consists of a Bruker 380E Pulsed EPR Spectrometer with pulsed ENDOR and has been modified to include pulsed ELDOR capabilities.

	Varian INOVA 800 The Varian 800 is an INOVA based spectrometer and an Oxford 18.8 T magnet with a 63 mm room temperature bore. This system is capable of high resolution liquid and solid state NMR. There are 4 RF channels with waveform generators and pulsed field gradients. The wideline ADC's run at 5 MHz and the narrow ADC's have a maximum rate of 500 kHz. We currently have a 5 mm HCN probe with Z-gradient for liquids and a single tuned 5 mm MAS probe. Under construction are a 5 mm orthogonal powder probe optimized for low gamma nuclides, a 5 mm HX MAS probe (12 kHz spinning), and a 4 mm HXY MAS probe (25 kHz spinning).
Varian INOVA 750 The Varian 750 is an INOVA based spectrometer and an Oxford 17.6 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquids, solid state NMR and µ-imaging. There are 4 RF channels with waveform generators and pulsed field gradients. The narrow ADC's have a maximum rate of 500 kHz. We currently have two 5 mm HCN probes (Z-gradient), an 8 mm HCN probe (Z-gradient), a 5 mm HCP probe (Z-gradient), a 5 mm HX MAS probe (10 kHz spinning) and a µ-imaging probe.
	Varian INOVA 600 The Varian 600 is an INOVA based spectrometer and an Oxford 14.1 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquid. There are 4 RF channels with waveform generators and pulsed field gradients. The narrow ADC's have a maximum rate of 500 kHz. We currently have a 5 mm HCN probe with Z-gradient and a 5 mm HX probe.
Varian Unity 600 The Varian 600 is an Unity based spectrometer and an Oxford 14.1 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquid. There are 3 RF channels with waveform generators and pulsed field gradients. The narrow ADC's have a maximum rate of 500 kHz. We currently have a 5 mm HCN probe with Z-gradient and a 5 mm HX probe.
	Varian Unity+ 500 The Varian 500 is an Unity+ based spectrometer and an Oxford 11.7 T magnet with a 89 mm room temperature bore. This system is capable of solid state NMR, µ-imaging and small animal MRI. There are 3 RF channels with waveform generators. The wideline ADC's run at 5 MHz. We currently have a 5 mm orthogonal powder probe, 5 mm HXY MAS probe (15 kHz spinning), a 7 mm HX MAS probe (10 kHz spinning), an HX single crystal probe, a 1H CRAMPS probe, a micro-coil imaging probe, and a 40 mm imaging probe. Under construction are a combined µ-imaging and optical microscope probe and a static HX low temperature probe (2 - 300 K).
Varian/Chemagnetics Infinity 500 The Chemagnetics 500 is an Infinity based spectrometer and an Oxford 11.7 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquid and solid state NMR. There are 3 RF channels. We currently have a 5 mm HCN probe, a 10 mm HX probe, and a 5 mm HX MAS probe.
	Varian Unity+ 500 The Varian 500 is an Unity+ based spectrometer and an Oxford 11.7 T magnet with a 51 mm room temperature bore. This system is capable of high resolution liquids NMR. There are 3 RF channels with waveform generators and pulsed field gradients. We currently have a 5 mm HCN probe with Z-gradient and a 10 mm HX probe.
Homebuilt/Tecmag 400 The homebuilt 400 spectrometer is based on homebuilt transmitter/receiver RF sections, a Tecmag pulse programmer and signal averager, and an Oxford 9.4 T magnet with a 89 mm room temperature bore. This system is capable of solid state NMR. There are 2 RF channels and 4 MHz ADC's. We currently have a 5 mm orthogonal powder probe, a 5 mm HX static low temperature probe (3.8 - 300 K), a 7 mm HX static low temperature probe (4.2 - 400 K), a 10 mm HX DAS probe.
	Varian/Chemagnetics Infinity 300 The Chemagnetics 300 is an Infinity based spectrometer and an Oxford 7.04 T magnet with a 89 mm room temperature bore. This system is capable of high resolution liquid and solid state NMR. There are 3 RF channels. We currently have a 5 mm HX probe, a 10 mm HX probe, a 7.5 mm HX MAS probe, and a 5 mm orthogonal powder probe.
Varian Unity+ 300 The Varian 300 is an Unity+ based spectrometer and an Oxford 7.04 T magnet with a 89 mm room temperature bore. This system is capable of solid state NMR, µ-imaging and small animal MRI. There are 2 RF channels with wideline ADC's running at 5 MHz. We currently have a 7 mm HX MAS probe (10 kHz spinning), an HX single crystal probe, a 1H CRAMPS probe, a single tuned DOR probe, an HX 5mm low temperature MAS probe (35-300K, 12 kHz spinning), a 7 mm HX High temperature probe (-100 - 500°C, 7 kHz spinning), a microscopy probe and a 40 mm imaging probe.
	Bruker Pulsed EPR/ENDOR/ELDOR Spectrometer The EPR/ENDOR work focuses on the development and application of pulsed-2D methods for electronic structure and distance determinations in biological macromolecules and materials. The spectrometer consists of a Bruker 380E Pulsed EPR Spectrometer with pulsed ENDOR and has been modified to include pulsed ELDOR capabilities.