Virtual Laboratory



Web Based Remote Control of Neutron Scattering Instruments
at ORNL's High Flux Isotope Reactor (HFIR)

LDRD Research Inititive

Why DIXIE Was Selected
For Initial Remote Implementation

A medium-resolution double-crystal small-angle neutron scattering (DIXIE) instrument has been completed and is in the initial testing phase. This instrument uses two spherically bent silicon crystals as monochromator and analyzer. The bent crystals coarsen the resolution while dramatically improving the peak intensity. The curvature of these crystals has the added benefit of focusing the beam spatially, which allows the use of small samples. In its current geometry, the Q-resolution is 0.0008Å-1. A Q of 0.001Å-1 corresponds to structures greater than 6000Å in size. The resolution and degree of spatial focusing can be varied, although not continuously, with the choice of analyzer reflection, curvature of the crystals and monochromator-analyzer distance. The DIXIE is equipped with motion controllers, computer and GPIB interface and all the accoutrements necessary to perform experiments on materials of interest. Currently, a commercial instrument control package, Labview, is used to run the machine. This proposal is not intended to build a new machine. The fully functional machine already exists. Experiments cannot, however, be run remotely at the present time.

The DIXIE is a good choice because it small and there is no need or chance for the remote user to move large pieces of shielding. Any runaway motions caused in the testing phases have very little potential for irrevocable damage. Another reason for the choice of instrument is that it has not yet developed a large user base and interruptions to its operations will not impact the existing user program adversely. At the same time, small-angle scattering is a very popular technique and SANS instruments that are in operation are heavily oversubscribed. Hence, when the project is completed, the potential number of researchers that will welcome the opportunity to visit the virtual laboratory will be substantial. Lastly, data files produced by the DIXIE are relatively small and will not need very much effort to archive and distribute effectively.