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Materials for Sample Preparation

A list of equipment and materials necessary for preparation of polished specimens is given in Table 1. For some items, substitution may be possible if comparable supplies are available in the laboratory. The list is presented in order of use of the equipment or supplies.

 

Table 1. Equipment and Supplies for Preparation of Polished Sections

Item Purpose

Diamond blade slab sawlarge-sized sample slabbing
Diamond blade wafering sawcutting of thin (mm-sized) sections
Propylene glycoldiamond saw cutting lubricant
Alcohol: 200 proof ethanolcutting lubricant, cleaning aid
Ultrasonic bathspecimen cleaning
Specimen jars and lidsfor replacement steps
Potting epoxies (medium and low viscosity) for powders and hardened pastes
Dye, blue or red, alcohol miscible to estimate alcohol replacement depth
Refrigeratorepoxy storage
Vacuum chamber and pumpvacuum impregnation
Drying / curing ovencapable of at least 65 ºC
Glass plate (400 x 400 mm)smooth surface for grinding
Lapidary wheel (minimum 200 mm) grinding and polishing
Mold cupspotting specimens
Aluminum foil (extra heavy duty)for forming odd-sized specimen molds
Mold releasefacilitates removal of specimen / epoxy
Metal trays to hold specimens contains any leaking epoxy
Diamond penlabel engraving
Abrasive papers (silicon carbide) coarse to fine grinding, 100 to 600 grit
Polishing cloths (low-relief) µm and finer polishing
Diamond paste for polishing 6, 3, 1, 0.25 µm in non-aqueous suspension
Lint-free clothsspecimen handling and cleaning
Compressed airspecimen cleaning and drying
Vacuum dessiccatorsspecimen storage

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Polished Powder Mounts Up: Main Previous: Introduction