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Title	Development of nondestructive evaluation methods for ceramic coatings.
Creator/Author	Ellingson, W. A. ; Deemer, C. ; Sun, J. G. ; Erdman, S. ; Muliere, D. ; Wheeler, B.
Publication Date	2002 Apr 29
OSTI Identifier	OSTI ID: 795035
Report Number(s)	ANL/ET/CP-107527
DOE Contract Number	W-31-109-ENG-38
Other Number(s)	TRN: US200215%%255
Resource Type	Conference
Resource Relation	16th Annual Conference on Fossil Energy Materials, Baltimore, MD (US), 04/22/2002--04/24/2002 ; PBD: 29 Apr 2002; PBD: 29 Apr 2002
Research Org	Argonne National Lab., IL (US)
Sponsoring Org	US Department of Energy (US)
Subject	20 FOSSIL-FUELED POWER PLANTS; 36 MATERIALS SCIENCE ; CERAMICS; COATINGS; COMBUSTORS; DEFECTS; EVALUATION; FIELD TESTS; OXIDES; THERMAL BARRIERS; TOPOGRAPHY; TURBINES; VANES
Description/Abstract	Various nondestructive evaluation (NDE) technologies are being developed to study the use of ceramic coatings on components in the hot-gas path of advanced low-emission gas-fired turbines. The types of ceramic coatings include thermal barrier coatings (TBCs) and environmental barrier coatings (EBCs). TBCs are under development for vanes, blades, and combustor liners to allow hotter gas-path temperatures, and EBCs are under development to reduce environmental damage to high-temperature components made of ceramic matrix composites. The NDE methods will be used to (a) provide data to assess the reliability of new coating application processes, (b) identify defective components that could cause unscheduled outages, (c) track growth rates of defects during component use in engines, and (d) allow rational judgment for replace/repair/re-use decisions regarding components. Advances in TBC application, both electron beam-physical vapor deposition (EB-PVD) and air plasma spraying (APS), are allowing higher temperatures in the hot-gas path. However, as TBCs become ''prime reliant,'' their condition at scheduled or unscheduled outages must be known. NDE methods are under development to assess the condition of the TBC for pre-spall conditions. EB-PVD test samples with up to 70 thermal cycles have been studied by a newly developed method involving polarized laser back-scatter NDE. Results suggest a correlation between the NDE laser data and the TBC/bond-coat topography. This finding is important because several theories directed toward understanding the pre-spall condition suggest that the topography in the thermally grown oxide layer changes significantly as a function of the number of thermal cycles. Tests have also been conducted with this NDE method on APS TBCs. Results suggest that the pre-spall condition is detected for these coatings. One-sided, high-speed thermal imaging also has shown promise for NDE of APS coatings. Testing of SiC/SiC composites for combustor liners has demonstrated that environmental EBCs are required to reduce oxidation-induced recession rates. NDE technologies, primarily one-sided and through-thickness thermal imaging, are under development to detect delaminations and degradation of EBCs. Recent results have demonstrated that NDE thermal image data correctly detected pre-spall regions of a barium-strontium-alumino-silicate coating on melt-infiltrated SiC/SiC. The NDE data were verified with field test data from a combustor liner in a 4.5 MW(e) natural-gas-fired turbine. The shape of the spalled EBC region and the growth of the spalled EBC region after various engine run times were correlated with boroscope image data from field tests. An effort has recently been started to address NDE development for oxide/oxide ceramic composites with an EBC. We will discuss the NDE methods under development for TBCs, recent NDE test results from thermally cycled TBCs, NDE results from EBCs on SiC/SiC, and the new effort directed toward oxide/oxide materials.
Country of Publication	United States
Language	English
Format	3 pages ; PDFN
System Entry Date	2002 Sep 02
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