The Microgravity Research Experiments (MICREX) Database


Fluid Physics


Liquid Floating Zone (SD20-TV101)


Principal Investigator(s):

Carruthers, J. (1)

Co-Investigator(s):

Bannister, T. (2)

Affiliations:

(1) During Skylab: Bell Laboratories, Murray Hill, New Jersey, Currently: INTEL, Santa Clara, California; (2) During Skylab: National Aeronautics and Space Administration (NASA), Marshall Space Flight Center (MSFC), Huntsville, Alabama, Currently: Boeing Aerospace, Huntsville, Alabama

Experiment Origin:

United States of America

Mission:

Skylab, SL-4, Third Skylab Manned Mission

LaunchDate/Experiment Date:

11/16/73

Launched From:

NASA Kennedy Space Center, Florida

Payload Type:

Science Demonstration, Skylab Manned Environment

Processing Facility:

Makeshift Floating Zone Apparatus

Builder of Processing Facility:

Astronaut Gibson

Experiment Summary:

Liquid Floating Zone (SD20-TV101)

The objective of this Skylab demonstration was to study the dynamic behavior of a column of liquid suspended between two aluminum discs. Such columns of liquid (better known as liquid bridges) are used to model the containerless float zone solidification geometry.

During the third manned Skylab mission, the make-shift liquid bridge apparatus was constructed using onboard equipment. Two socket wrench extension rods were configured in parallel such that a small gap existed between the two rods. At the ends of the rods forming the gap, circular aluminum discs were attached. "The front surfaces of the discs were coated with grey tape which had been previously treated by immersion in acetone so as to reduce the contact angle with water. During the course of the experiments, the outer edges of the discs were coated with Krytox oil to prevent capillary wetting of water in that region." (1, p. 843). The rods were mounted in camera mounts such that the assembly was free to rotate smoothly.

"Rotation of the zones was performed manually by first winding ... twine around the socket wrench and then withdrawing it at a uniform rate." (1, p. 843) Liquid bridges were created by (1) deploying a volume of fluid from a syringe on to each aluminum disc, (2) moving the discs close together to create one liquid volume, and (3) separating the discs to suspend the liquid into the desired column length. During 26 separate zone investigations, several water-based bridges were successfully formed, as bridge length, rotational direction, and bridge fluid were varied. Fluid additives such as rope particles aided internal fluid motion observance, while liquid soap was used to vary surface tension and viscosity. Video taping of most of these investigations was successfully achieved. Among the several observations of interest was the creation of a long, static, stable, unduloid bridge which exceeded the theoretical length limit for a right circular cylinder. When the liquid bridge was subjected to "...longitudinal vibrations of the end discs....standing waves occurred when the disc oscillation frequency coincided with a resonant frequency of the surface.

"When standing waves were produced, there was no transfer of liquid from one wave region to another inside the zone." (1, pp. 847-848) Rotation of the zone also resulted in some interesting observations. "For sequences involving the single rotation of only one bounding disc, the zone assumed an axisymmetric bottle shaped deformation possessing stability limits in general agreement with theory. For sequences involving equal rotation rates of both bounding discs, the zone becomes deformed in a non-axisymmetric fashion resembling a turning skipping rope [or C-mode] when the zone lengths exceed some value in the vicinity of...[(2/3)(pi)R]. Short zone lengths do not generally develop the rotating C-mode but do demonstrate capillary wave resonances presumably arising from nonparallel disc alignment." (2, p. 6)

Key Words:

*Fluid Physics*Liquid Columns*Liquid Bridges*Liquid Bridge Stability*Liquid Dynamic Response*Hydrodynamics*Liquid Vibration*Axial Oscillations*Oscillation Frequency*Resonant Frequency*Rotating Fluids*Sample Rotation*Liquid Expulsion Through a Small Orifice*Solid/Liquid Interface*Liquid/Gas Interface*Free Surface*Surface Tension*Viscosity*Wetting*Contact Angle*Capillary Forces*Coated Surfaces*Containerless Processing Applications*

Number of Samples:

A total of 26 experimental runs were realized.

Sample Materials:

Most of the zones were water based. Additives such as rope particles and soap were used for some runs. Soap solution and soap foam liquid bridges were also formed.

Container Materials:

not applicable

Experiment/Material Applications:

These liquid bridge experiments demonstrated some of the fluid dynamic characteristics of reduced gravity bridge formation and rotation. Such bridge formation and rotation characteristics are of interest for floating zone crystal growth. Float zone materials processing is a popular method of growing semiconductors crystals in industry. However, the maximum length of the zone in 1-g is limited by the balance of hydrostatic pressure with the liquid surface tension.

References/Applicable Publications:

(1) Carruthers, J. R.: Studies of Liquid Floating Zones in SL-IV, the Third Skylab Mission. In Marshall Space Flight Center Proceedings of the Third Space Processing Symposium on Skylab Results, Vol. 2, June 1974, pp. 837-856. (post-flight)

(2) Carruthers, J. R., Gibson, E. G., Klett, M. G., and Facemire, B.: Studies of Rotating Liquid Floating Zones on Skylab IV. American Institute of Aeronautics and Astronautics, 10th Thermophysics Conference, Denver, Colorado, May 27-29, 1975, AIAA Paper #75-692, 8 pp.

(3) Chassay, R. P. and Schwaniger, A.: Low G Measurements at NASA. In Workshop Proceedings of the Measurement and Characterization of the Acceleration Environment on Board the Space Station, August 11-14, 1986, Guntersville, Alabama, p. 9-1. (acceleration measurements)

(4) TV101-Liquid Floating Zone. In MSFC Skylab Corollary Experiment Systems Mission Evaluation, NASA TM X-64820, September 1974, pp. 7-4 - 7-10. (post-flight)

(5) Naumann, R. J. and Herring, H. W.: Experiment TV101, Liquid Floating Zone. In Materials and Processing in Space: Early Experiments, NASA SP-443, 1980, pp. 79-81. (post-flight)

(6) Bannister, T. C.: Science Demonstrations on Skylab in the Material Processing Area. In Proceedings of the Third Space Processing Symposium on Skylab Results, April 30-May 1, 1974, Marshall Space Flight Center, Huntsville, Alabama, Vol. 1, June 1974, pp. 491-505. (post-flight)

(7) Bannister, T. C.: Skylab III and IV Science Demonstrations. NASA TM X-64835, March 1974, pp. 6-8. (post-flight)

(8) Naumann, R. J. and Mason, E. D.: Liquid Floating Zone. In Summaries of Early Materials Processing in Space Experiments, NASA TM-78240, August 1979, pp. 40-41. (post-flight)

(9) Liquid Floating Zone (SD20-TV101). In MSFC Skylab Mission Report-Saturn Workshop, NASA TM X-64814, October 1974, pp. 12-89 - 12-90.

(10) Input received from Principal Investigator John Carruthers, June 1993.

Contact(s):

John Carruthers
INTEL
2250 Mission College Blvd.
Mail Stop SC1-02
P.O. Box 58125
Santa Clara, CA 95052-8125