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***************** NEW DISSOLVED GAS SYSTEM -- For Serum Bottles
************************** |
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| Program
written by E. Busenberg, USGS,
(8-30-1994), Rev. (12/07/2001) |
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| This
program calculates the dissolved gas composition of waters, and the volume
percent composition in a gas sample.. |
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| Henry's law constants were
obtained from: |
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| R.
F. Weiss, 1970, Deep-Sea Res., vol. 17, 721-735. |
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| E.
Wilhelm et al., 1977, Chem. Rev., vol. 77, 219-262. |
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| Samples submitted by: |
L. H. |
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| District: |
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| Geographic
location: |
Florida Samples |
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| Date
received: |
6/14/2004 |
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| Date
analyzed: |
7/23/2004 |
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| Analyzed by: |
PW |
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| Comments:
(worksheet): |
FL-L H-2004 |
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| Barometic Pressure
Uncorrected: |
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750.85 |
mm Hg |
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| Initial Room
Temperature: |
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25.2 |
C |
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| Final Room
Temperature: |
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25.5 |
C |
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| Percent
Relative Humidity: |
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45.5 |
% |
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| Barometric
Pressure: |
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747.65 |
mm Hg |
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| Room
Temperature in Kelvin: |
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298.5 |
K |
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Bottle Weights |
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Field |
Density |
Field |
Ionic |
Salinity |
Chlorinity |
Elevation |
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| Sample |
Empty Wt |
Full Wt |
Hdsp Wt |
Temp. |
Water |
DO |
Strength |
in o/oo |
in o/oo |
in feet |
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| Quality Control 2004 Q243 |
104.22 |
263.42 |
253.23 |
27 |
0.997 |
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| Quality
Control 2004 Q247 |
104.6 |
263.36 |
253.01 |
16.7 |
0.997 |
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| Clear Spring
5/25/04 1255 4A0890 |
102.78 |
262.13 |
251.76 |
23 |
0.997 |
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| Clear Spring
6/11/04 1435 4A0881 |
105.18 |
264.2 |
254.26 |
23 |
0.997 |
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| Cutwater
6/12/04 1600 4A0887 |
104.57 |
263.71 |
254.13 |
23 |
0.997 |
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| Cutwater
5/14/04 1400 4A0888 |
104.91 |
263.42 |
253.55 |
23 |
0.997 |
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| Kentwell
Spring #1 5/18/04 1600 4A0889 |
105.24 |
263.39 |
253.19 |
23 |
0.997 |
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| Old Mill
6/21/04 1600 4A0174 |
102.76 |
263.02 |
253.21 |
21.57 |
0.997 |
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| Main Spring
House 6/30/2004 1500 4A0154 |
101.37 |
263 |
253.09 |
20.9 |
0.997 |
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| Emerson
Spring 6/23/2004 1500 4A0161 |
103.59 |
262.72 |
252.65 |
21.3 |
0.997 |
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| Main Spring
House 4/26/2004 1430 4A0156 |
102.49 |
262.23 |
250.16 |
20.8 |
0.997 |
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| Alderman
Spring 6/23/04 1700 4A0169 |
103.04 |
262.25 |
252.58 |
22.12 |
0.997 |
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| Lowry Spring
6/23/04 1600 4A0175 |
103.38 |
262.79 |
253.47 |
22.06 |
0.997 |
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| Quality
Control 2004 Q253 |
104.58 |
263.37 |
252.95 |
9.3 |
0.997 |
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| -------- COMPOSITION OF
STANDARDS ---------- |
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| Standard |
O2 |
CH4 |
CO2 |
N2 |
Ar + O2 |
Ar |
CH4 |
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| AIR |
20.946 |
0 |
0 |
78.084 |
21.88 |
0.934 |
0 |
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| C1 Std-1 |
0 |
4.92 |
10 |
84.03 |
1.05 |
1.05 |
4.92 |
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| C1 Std-2 |
0 |
1.05 |
1.02 |
97.93 |
0 |
0 |
1.05 |
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| C3 Std-3 |
10.02 |
0 |
0 |
87.97 |
12.03 |
2.01 |
0 |
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| C3 Std-2 |
20.618 |
0 |
0 |
78.369 |
21.631 |
1.013 |
0 |
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Transducer Volt Readings |
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BPU(-3.2) |
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Areas from Integrator |
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| Initial
Standards |
V(vac.) |
V(total)
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V(inject) |
V(air) |
Reading |
CH4 (i) |
CO2(i) |
CH4 (o) |
Ar(i) |
N2(i) |
Ar + O2(o) |
N2(o) |
|
| Air |
0.7299 |
1.4036 |
0.9695 |
3.6591 |
750.7 |
0 |
0 |
0 |
161654 |
12430326 |
6360615 |
24168786 |
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| C3 Std-3 (1) |
0.7299 |
1.5963 |
1.0365 |
3.6676 |
750.7 |
0 |
0 |
0 |
453605 |
18001260 |
4578152 |
34966179 |
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| C3 Std-3 (2) |
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0 |
0 |
0 |
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| C3 Std-2 (1) |
0.7295 |
1.4167 |
0.9757 |
3.6596 |
750.7 |
0 |
0 |
0 |
182301 |
12831772 |
6455243 |
25001321 |
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| C3 Std-2 (2) |
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0 |
0 |
0 |
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| C1 Std-1 (1) |
0.7299 |
1.4107 |
0.974 |
3.6599 |
750.7 |
2639719 |
5121928 |
4199597 |
0 |
13659217 |
0 |
26703953 |
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| C1 Std-1 (2) |
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0 |
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0 |
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| C1 Std-2 (1) |
0.7297 |
1.4325 |
0.9798 |
3.6599 |
750.7 |
574123 |
525265 |
912987 |
0 |
16291633 |
0 |
31715844 |
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| C1 Std-2 (2) |
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0 |
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0 |
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| Final Standards |
V(vac.) |
V(total) |
V(inject) |
V(air) |
BPU |
CH4 (i) |
CO2(i) |
CH4 (o) |
Ar(i) |
N2(i) |
Ar + O2(o) |
N2(o) |
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| C3 Std-3 |
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0 |
0 |
0 |
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| C3 Std-2 |
0.7315 |
1.4135 |
0.9737 |
3.6699 |
751 |
0 |
0 |
0 |
179154 |
12722409 |
6417233 |
24740668 |
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| C1 Std-1 |
0.7315 |
1.4047 |
0.9741 |
3.6588 |
751 |
2658736 |
5180582 |
4217587 |
0 |
13617745 |
0 |
26716337 |
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| C1 Std-2 |
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0 |
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0 |
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| *** STANDARDS *** |
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|
volts/atm. |
|
CH4 (i) |
CO2(i) |
CH4 (o) |
Ar (i) |
N2(i) |
Ar + O2 (o) |
N2 (o) |
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| No. of standards |
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|
7 |
|
3 |
3 |
3 |
4 |
7 |
4 |
7 |
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| Mean |
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2.980529 |
|
656884092 |
625192872 |
1043881602 |
217546599 |
198683948 |
364484210.8 |
387248415 |
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| Standard
Deviation |
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|
0.004378 |
|
6334842.7 |
11387463 |
8593419.37 |
1685625.1 |
618414.64 |
4029655.97 |
1908231.7 |
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| % Standard
Deviation |
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0.146884 |
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0.9643776 |
1.8214321 |
0.82321782 |
0.774834 |
0.3112555 |
1.105577649 |
0.4927668 |
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Analysis |
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| ***** SAMPLES ***** |
Transducer Volt Readings |
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Temp |
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Areas from Integrator |
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| Well Name |
V(vac.) |
V(total)
|
V(inject) |
V(air) |
of sample |
CH4 (i) |
CO2(i) |
CH4 (o) |
Ar(i) |
N2(i) |
Ar + O2(o) |
N2(o) |
CO(o) |
| Quality Control 2004 Q243 |
0.7291 |
1.2481 |
0.914 |
3.6634 |
24.6 |
|
63147 |
|
187210 |
8146389 |
6707497 |
15877797 |
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| Quality
Control 2004 Q247 |
0.7296 |
1.339 |
0.9443 |
3.6643 |
24.6 |
|
85091 |
|
221660 |
9411757 |
8020879 |
18329307 |
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| Clear Spring
5/25/04 1255 4A0890 |
0.7319 |
1.217 |
1.0882 |
3.6624 |
24.6 |
|
2543872 |
|
443914 |
21073154 |
845428 |
40950697 |
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| Clear Spring
6/11/04 1435 4A0881 |
0.7301 |
1.2315 |
0.9085 |
3.6599 |
24.6 |
|
1292268 |
|
225951 |
10806819 |
420509 |
21071735 |
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| Cutwater
6/12/04 1600 4A0887 |
0.7287 |
1.2484 |
0.9121 |
3.6596 |
24.6 |
|
1240934 |
|
230783 |
11474334 |
422792 |
22020312 |
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| Cutwater
5/14/04 1400 4A0888 |
0.7293 |
1.2344 |
0.9096 |
3.6585 |
24.6 |
|
1271989 |
|
225397 |
10956799 |
419649 |
21351955 |
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| Kentwell
Spring #1 5/18/04 1600 4A0889 |
0.7312 |
1.2351 |
0.9101 |
3.6589 |
24.6 |
499312 |
1208365 |
799687 |
221493 |
10798914 |
512124 |
21065085 |
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| Old Mill
6/21/04 1600 4A0174 |
0.7294 |
1.3078 |
0.9357 |
3.6594 |
24.8 |
|
3459227 |
|
224147 |
10247687 |
3549016 |
20086873 |
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| Main Spring
House 6/30/2004 1500 4A0154 |
0.7307 |
1.3133 |
0.9378 |
3.659 |
24.8 |
|
4046756 |
|
225730 |
10237360 |
3500336 |
20028552 |
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| Emerson Spring
6/23/2004 1500 4A0161 |
0.7298 |
1.3428 |
0.9479 |
3.6582 |
24.8 |
|
4893869 |
|
225789 |
10181092 |
4289122 |
19958093 |
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| Main Spring
House 4/26/2004 1430 4A0156 |
0.7302 |
1.2508 |
0.915 |
3.6589 |
24.8 |
|
3756416 |
|
203832 |
8808845 |
3283156 |
17273502 |
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| Alderman
Spring 6/23/04 1700 4A0169 |
0.7304 |
1.3001 |
0.9322 |
3.659 |
24.8 |
|
4296086 |
|
212863 |
9700759 |
3433984 |
19039658 |
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| Lowry Spring
6/23/04 1600 4A0175 |
0.7303 |
1.3154 |
0.9391 |
3.6567 |
24.8 |
|
3472433 |
|
225762 |
10415834 |
3544988 |
20403059 |
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| Quality
Control 2004 Q253 |
0.7313 |
1.423 |
0.9755 |
3.6622 |
24.8 |
|
101527 |
|
255425 |
10713123 |
9259465 |
20858603 |
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| ***** SAMPLES ***** |
Sum |
Sidearm |
Sum |
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Partial pressure of gases in
bottle at bottle temperature (Analysis) |
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Corr. Expans. |
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| Well Name |
Pres. |
Pressure |
N2+O2+Ar |
O2 by dif. |
CH4(1) |
CO2 |
N2 |
O2+Ar |
Ar |
CH4(2) |
H2O |
|
| Quality Control 2004 Q243 |
0.22916667 |
0.236135 |
0.2011929 |
0.058564 |
0 |
0.0003372 |
0.1368829 |
0.06143706 |
0.0028729 |
0 |
0.027636563 |
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| Quality
Control 2004 Q247 |
0.26993803 |
0.276139 |
0.2417933 |
0.072126 |
0 |
0.0004677 |
0.1626643 |
0.07562737 |
0.0035016 |
0 |
0.027677008 |
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| Clear Spring
5/25/04 1255 4A0890 |
0.21333687 |
0.219705 |
0.1790387 |
0.000454 |
0 |
0.0066162 |
0.1719491 |
0.0037716 |
0.003318 |
0 |
0.027681984 |
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| Clear Spring
6/11/04 1435 4A0881 |
0.22302908 |
0.229634 |
0.1885723 |
0.000383 |
0 |
0.0068858 |
0.181269 |
0.00384335 |
0.00346 |
0 |
0.027571014 |
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| Cutwater
6/12/04 1600 4A0887 |
0.23358204 |
0.240406 |
0.1994118 |
0.000335 |
0 |
0.006699 |
0.1919164 |
0.00391495 |
0.0035804 |
0 |
0.027471214 |
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| Cutwater
5/14/04 1400 4A0888 |
0.22508577 |
0.231767 |
0.1907632 |
0.000384 |
0 |
0.0067705 |
0.1834839 |
0.0038314 |
0.0034478 |
0 |
0.027552123 |
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| Kentwell
Spring #1 5/18/04 1600 4A0889 |
0.22368888 |
0.229205 |
0.1862446 |
0.001268 |
0.00347 |
0.0063353 |
0.1783018 |
0.00460552 |
0.0033373 |
0.002511 |
0.027639125 |
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| Old Mill
6/21/04 1600 4A0174 |
0.25902361 |
0.265837 |
0.2123953 |
0.029523 |
0 |
0.0187616 |
0.1758848 |
0.03301679 |
0.0034937 |
0 |
0.027866721 |
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| Main Spring
House 6/30/2004 1500 4A0154 |
0.26032838 |
0.267038 |
0.2105772 |
0.028925 |
0 |
0.0218569 |
0.1746449 |
0.03242852 |
0.0035037 |
0 |
0.027894258 |
|
| Emerson Spring
6/23/2004 1500 4A0161 |
0.27323654 |
0.279775 |
0.2186939 |
0.036469 |
0 |
0.0266053 |
0.17517 |
0.03999632 |
0.0035276 |
0 |
0.027937289 |
|
| Main Spring
House 4/26/2004 1430 4A0156 |
0.22163139 |
0.227175 |
0.1740717 |
0.025754 |
0 |
0.019173 |
0.1423381 |
0.02874373 |
0.0029899 |
0 |
0.02838671 |
|
| Alderman
Spring 6/23/04 1700 4A0169 |
0.25577758 |
0.262862 |
0.2043736 |
0.028968 |
0 |
0.0235766 |
0.1686912 |
0.03232529 |
0.0033572 |
0 |
0.027827307 |
|
| Lowry Spring
6/23/04 1600 4A0175 |
0.26551646 |
0.272734 |
0.2186526 |
0.02994 |
0 |
0.0191397 |
0.1815605 |
0.03351597 |
0.0035761 |
0 |
0.027724122 |
|
| Quality
Control 2004 Q253 |
0.30719234 |
0.312886 |
0.2786027 |
0.083919 |
0 |
0.0005624 |
0.1865511 |
0.08798515 |
0.0040664 |
0 |
0.028027238 |
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| ***** SAMPLES ***** |
|
Concentration in mg/L |
|
|
Concentration in mmol/L |
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|
| Well Name |
CH4 |
CO2 |
N2 |
O2 |
Ar |
CH4 |
CO2 |
N2 |
O2 |
Ar |
|
| Quality Control 2004 Q243 |
0 |
0.549136 |
13.235111 |
7.643274 |
0.482071 |
0 |
0.0124775 |
0.47246318 |
0.2388598 |
0.0120675 |
|
| Quality
Control 2004 Q247 |
0 |
0.762865 |
15.980524 |
9.541173 |
0.595321 |
0 |
0.0173339 |
0.57046815 |
0.298171 |
0.0149024 |
|
| Clear Spring
5/25/04 1255 4A0890 |
0 |
10.78918 |
16.866548 |
0.059928 |
0.56338 |
0 |
0.2451529 |
0.60209718 |
0.0018728 |
0.0141028 |
|
| Clear Spring
6/11/04 1435 4A0881 |
0 |
11.19237 |
17.171563 |
0.049174 |
0.570909 |
0 |
0.2543142 |
0.61298552 |
0.0015367 |
0.0142913 |
|
| Cutwater
6/12/04 1600 4A0887 |
0 |
10.85726 |
17.603448 |
0.041767 |
0.575431 |
0 |
0.2466998 |
0.6284028 |
0.0013053 |
0.0144045 |
|
| Cutwater
5/14/04 1400 4A0888 |
0 |
11.00166 |
17.323834 |
0.049064 |
0.567361 |
0 |
0.2499809 |
0.61842122 |
0.0015333 |
0.0142025 |
|
| Kentwell
Spring #1 5/18/04 1600 4A0889 |
0.23489012 |
10.32348 |
17.353853 |
0.166448 |
0.563026 |
0.0146413 |
0.2345713 |
0.61949284 |
0.0052017 |
0.014094 |
|
| Old Mill
6/21/04 1600 4A0174 |
0 |
30.29168 |
16.346692 |
3.724402 |
0.567156 |
0 |
0.6882909 |
0.58353951 |
0.1163912 |
0.0141973 |
|
| Main Spring
House 6/30/2004 1500 4A0154 |
0 |
35.29367 |
16.254135 |
3.653213 |
0.569435 |
0 |
0.8019465 |
0.58023542 |
0.1141665 |
0.0142544 |
|
| Emerson Spring
6/23/2004 1500 4A0161 |
0 |
43.06842 |
16.752388 |
4.712886 |
0.586219 |
0 |
0.9786054 |
0.59802191 |
0.1472823 |
0.0146745 |
|
| Main Spring
House 4/26/2004 1430 4A0156 |
0 |
31.52643 |
15.925059 |
3.806156 |
0.566126 |
0 |
0.716347 |
0.56848817 |
0.1189461 |
0.0141716 |
|
| Alderman
Spring 6/23/04 1700 4A0169 |
0 |
38.04288 |
15.573862 |
3.633944 |
0.542029 |
0 |
0.8644145 |
0.55595125 |
0.1135643 |
0.0135684 |
|
| Lowry Spring
6/23/04 1600 4A0175 |
0 |
30.79504 |
16.22757 |
3.655173 |
0.562375 |
0 |
0.6997282 |
0.57928712 |
0.1142277 |
0.0140777 |
|
| Quality
Control 2004 Q253 |
0 |
0.913165 |
18.4122 |
11.1385 |
0.693521 |
0 |
0.020749 |
0.65727342 |
0.3480891 |
0.0173606 |
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| |
Partial pressures at Field
Temperatures in atm. |
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|
Measured |
Tot Press |
|
|
| Well Name |
CH4 |
CO2 |
N2 |
O2 |
Ar |
Pressure |
Corrected |
|
|
| Quality Control 2004 Q243 |
0 |
0.000389 |
0.7488135 |
0.194099 |
0.008961 |
0.9522622 |
0.9522622 |
|
|
| Quality
Control 2004 Q247 |
0 |
0.000403 |
0.7696626 |
0.201744 |
0.009194 |
0.9810048 |
0.9810048 |
|
|
| Clear Spring
5/25/04 1255 4A0890 |
0 |
0.006858 |
0.9009213 |
0.001424 |
0.009789 |
0.9189926 |
0.9189926 |
|
|
| Clear Spring
6/11/04 1435 4A0881 |
0 |
0.007115 |
0.9172135 |
0.001169 |
0.00992 |
0.9354165 |
0.9354165 |
|
|
| Cutwater
6/12/04 1600 4A0887 |
0 |
0.006902 |
0.9402825 |
0.000993 |
0.009998 |
0.9581749 |
0.9581749 |
|
|
| Cutwater
5/14/04 1400 4A0888 |
0 |
0.006994 |
0.925347 |
0.001166 |
0.009858 |
0.9433644 |
0.9433644 |
|
|
| Kentwell
Spring #1 5/18/04 1600 4A0889 |
0.01015475 |
0.006562 |
0.9269505 |
0.003956 |
0.009783 |
0.9574059 |
0.9574059 |
|
|
| Old Mill
6/21/04 1600 4A0174 |
0 |
0.018496 |
0.8540854 |
0.086313 |
0.009606 |
0.9685005 |
0.9685005 |
|
|
| Main Spring
House 6/30/2004 1500 4A0154 |
0 |
0.021141 |
0.8402731 |
0.083648 |
0.009528 |
0.9545904 |
0.9545904 |
|
|
| Emerson Spring
6/23/2004 1500 4A0161 |
0 |
0.026095 |
0.8715611 |
0.108694 |
0.009881 |
1.0162311 |
1.0162311 |
|
|
| Main Spring
House 4/26/2004 1430 4A0156 |
0 |
0.01883 |
0.8219439 |
0.086992 |
0.009456 |
0.9372216 |
0.9372216 |
|
|
| Alderman
Spring 6/23/04 1700 4A0169 |
0 |
0.023594 |
0.820725 |
0.085043 |
0.009272 |
0.9386339 |
0.9386339 |
|
|
| Lowry Spring
6/23/04 1600 4A0175 |
0 |
0.019066 |
0.8543788 |
0.085449 |
0.00961 |
0.9685043 |
0.9685043 |
|
|
| Quality
Control 2004 Q253 |
0 |
0.00038 |
0.7684559 |
0.201088 |
0.009148 |
0.9790724 |
0.9790724 |
|
|
|
|
|
|
|
| |
Headspace -- Total
Amount in mmol |
|
|
|
|
Water -- Total Amount in mmol |
|
|
|
|
|
| Well Name |
CH4 |
CO2 |
N2 |
O2 |
Ar |
CH4 |
CO2 |
N2 |
O2 |
Ar |
|
| Quality Control 2004 Q243 |
0 |
0.000141 |
0.057262 |
0.024499 |
0.001202 |
0 |
0.0017238 |
0.01335163 |
0.0112006 |
0.0006018 |
|
| Quality
Control 2004 Q247 |
0 |
0.000199 |
0.0691155 |
0.030646 |
0.001488 |
0 |
0.0023815 |
0.01580246 |
0.0137387 |
0.0007305 |
|
| Clear Spring
5/25/04 1255 4A0890 |
0 |
0.002817 |
0.0732017 |
0.000193 |
0.001413 |
0 |
0.0338161 |
0.01676862 |
8.674E-05 |
0.0006948 |
|
| Clear Spring
6/11/04 1435 4A0881 |
0 |
0.00281 |
0.0739695 |
0.000156 |
0.001412 |
0 |
0.0352174 |
0.01768937 |
7.335E-05 |
0.0007251 |
|
| Cutwater
6/12/04 1600 4A0887 |
0 |
0.002635 |
0.075478 |
0.000132 |
0.001408 |
0 |
0.0343728 |
0.01878872 |
6.422E-05 |
0.0007527 |
|
| Cutwater
5/14/04 1400 4A0888 |
0 |
0.002743 |
0.0743461 |
0.000155 |
0.001397 |
0 |
0.0345256 |
0.01785267 |
7.318E-05 |
0.0007204 |
|
| Kentwell
Spring #1 5/18/04 1600 4A0889 |
0.00145298 |
0.002653 |
0.0746618 |
0.000531 |
0.001397 |
0.0007197 |
0.0321564 |
0.01726793 |
0.0002408 |
0.000694 |
|
| Old Mill
6/21/04 1600 4A0174 |
0 |
0.007551 |
0.0707862 |
0.011882 |
0.001406 |
0 |
0.0963142 |
0.01727153 |
0.005682 |
0.0007364 |
|
| Main Spring
House 6/30/2004 1500 4A0154 |
0 |
0.008886 |
0.0710037 |
0.01176 |
0.001424 |
0 |
0.1131513 |
0.01729455 |
0.0056138 |
0.0007447 |
|
| Emerson Spring
6/23/2004 1500 4A0161 |
0 |
0.010991 |
0.072367 |
0.015066 |
0.001457 |
0 |
0.1353185 |
0.01704242 |
0.0069539 |
0.0007366 |
|
| Main Spring
House 4/26/2004 1430 4A0156 |
0 |
0.009494 |
0.0704822 |
0.012753 |
0.001481 |
0 |
0.0966073 |
0.01371904 |
0.004865 |
0.0006185 |
|
| Alderman
Spring 6/23/04 1700 4A0169 |
0 |
0.009353 |
0.0669222 |
0.011492 |
0.001332 |
0 |
0.1203003 |
0.01646494 |
0.0055414 |
0.0007033 |
|
| Lowry Spring
6/23/04 1600 4A0175 |
0 |
0.007318 |
0.0694206 |
0.011448 |
0.001367 |
0 |
0.0980201 |
0.01778622 |
0.0057484 |
0.0007519 |
|
| Quality
Control 2004 Q253 |
0 |
0.00024 |
0.0797474 |
0.035874 |
0.001738 |
0 |
0.0028474 |
0.01806568 |
0.0159276 |
0.0008452 |
|
|
|
|
|
|
|
|
|
|
|
|
|
|
|