Polymers Main Page > Staff
Directory > Detail..Mark A. Arnould , Ph.D. |
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Research Chemist, MALDI Mass SpectrometryCharacterization and Measurement |
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Phone:
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(301) 975-6790
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Fax:
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(301) 976-3928
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Email:
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Mail:
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8541
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Research InterestsStructural and compositional characterization of synthetic polymers by MALDI-TOF mass spectrometry and tandem mass spectrometry. Other interests include: the application of novel MALDI-TOF instrumentation, chemical modification of synthetic polymers for covalent cationization, understanding the MALDI process and gas phase ionization of polymer molecules using transition metal complexes.Professional BackgroundB.S. Chemistry, The University of Akron, 1998.Ph.D. Chemistry, The University of Akron, 2003. Dissertation title: Mass Spectrometric Studies of Synthetic Polymers. Honors and AwardsUndergraduate Analytical Chemist Award, 1998.B.F. Goodrich Research Award, 2000. DIanni Fellowship, 1998-2000. ASMS Travel Award, 49th ASMS Conference, May 27-31, 2001, Chicago, IL. National Research Council post-doctoral fellowship at the National Institute of Standards and Technology, 2003. PublicationsWesdemiotis, C.; Arnould, M. A.; Lee, Y.; Quirk, R. P. MALDI TOF Mass Spectrometry of the Products from Novel Anionic Polymerizations, Polym. Prepr. 2000, 41(1), 629-630.Quirk, R. P.; Ge, Q.; Arnould, M. A.; Wesdemiotis, C. Functionalization of Poly(styryl)lithium with1-Butene Oxide, Macromol. Chem. Phys. 2001, 202, 1761-1767. Quirk, R. P.; Mathers, R. T.; Wesdemiotis, C.; Arnould, M. A. Investigation of Ethylene Oxide Oligomerization during Functionalization of Poly(styryl)lithium using MALDI-TOF MS and NMR, Macromolecules. 2002, 35, 2912-2918. Quirk, R. P.; Gomochak, D. L.; Wesdemiotis, C.; Arnould, M. A. Synthesis of Diene- Functionalized Macromonomers via Functionalization of Polymeric organolithiums with 3,4-epoxy-1-butene, Polym. Mat. Sci. & Eng. 2002, 87, 160-161. Quirk, R. P.; Mathers, R. T.; Ma, J.J.; Wesdemiotis, C.; Arnould, M. A. Reaction of Polymeric Organolithium Compounds with Ethylene Oxide in Hydrocarbon Solution: Determination of extent of Oligomerization, Macromol. Symp. 2002, 183, 17-22. Arnould, M. A.; Wesdemiotis, C.; Geiger, R. J.; Park, M. E.; Buehner, R. W.; Vandervost, D. Structural Characterization of Polyester Copolymers by MALDI Mass Spectrometry. Prog. Org. Coat. 2002, 45, 305-312. Quirk, R. P.; Guo, Ya.; Wesdemiotis, Chrys; Arnould, M. A. Functionalization of Polymeric Organolithium compounds with Formaldehyde. Polym. Mat. Sci. & Eng. 2003, 88, 542-543. Wesdemiotis, Chrys; Arnould, M. A.; Quirk, Roderic P. End Group Characterization in Anionic Polymerizations via Mass Spectrometry Methods. Polym. Mat. Sci. & Eng. 2003, 88, 130-131. Quirk, R. P.; Gomochak, Deanna L.; Wesdemiotis, Chrys; Arnould, M. A. Functionalization of Polymeric Organolithium Compounds with 3,4-epoxy-1-butene: Precursors for Diene-Functionalized Macromonomers. J. Polym. Sci., Part A: Polym. Chem. 2003, 41(7), 947-957 Quirk, R. P.; Guo, Ya.; Wesdemiotis, Chrys; Arnould, M. A. Functionalization of Polymeric Organolithium compounds with Formaldehyde. J. Polym. Sci. Polym. Chem. 2003, 41(16), 2435-2453 Quirk R.P.; Gomochak D.L.; Bhatia R.S.; Wesdemiotis C.; Arnould M.A.; Wollyung, K. Synthesis of diene-functionalized macromonomers via functionalization with hexa-1,3,5-triene. Macromol. Chem. Phys. 2003, 204, 2183-2196. Quirk, R.P.; You, F.; Wesdemiotis, C.; Arnould, M.A. Anionic Synthesis and Characterization of omega-Hydroxyl-Functionalized Poly(1,3-cyclohexadiene). Macromolecules 2004, 37, 1234-1242. Conferences31st Central Regional ACS Meeting, June 21-23, 1999 Columbus, OH. Talk: *Arnould, M. A.; Wesdemiotis, C.; Lee, y.; Quirk, R. P. MALDI-TOF Mass Spectrometric Analysis of Anionically Prepared Polystyrenes.1999 Ontario Gas Phase Ion Chemists Meeting, Trent University, October 29-30, 1999, Peterborough, Ontario, Canada. Talk: *Arnould, M. A.; Wesdemiotis, C. Compositional and Structural Analysis of Polymers by MALDI Mass Spectrometry. 219th National ACS Meeting, May 26-31, 2000, San Francisco, CA. Invited Talk: * Wesdemiotis, C.; Arnould, M. A.; Lee, y.; Quirk, R. P. MALDI-TOF Mass Spectrometry of the Products from Novel Anionic Polymerizations. 48th ASMS Conference, June 10-15, 2000, Long Beach, CA. Poster: * Arnould, M. A.; Wesdemiotis, C.; Lee, y.; Quirk, R. P. Product Analysis of Novel Anionic Polymerizations by MALDI-TOF MS. 2000 Ontario Gas Phase Ion Chemists Meeting, Trent University, October 29-30, 1999, Peterborough, Ontario, Canada. Talk: *Arnould, M. A.; Wesdemiotis, C. Composition and Sequence Characterization of Polyester Copolymers. 49th ASMS Conference, May 27-31, 2001, Chicago, IL. Talk: * Wesdemiotis, C; Arnould, M. A.; Cheong, T. H.; Quirk, R. P. The Use of Functional and Chain-extended Initiators in the Anionic Polymerization of Dienes. Talk: *Arnould, M. A.; Wesdemiotis, C. The Application of MALDI-TOF Tandem Mass Spectrometry in the Sequencing of Polyester Monomers. 2001 Athens Conference on coatings: Science and Technology, July 2-6, Vouliagmeni (Athens), Greece. Talk: *Wesdemiotis, C.; Arnould, M. A.; Geiger, R. J.; Park, M. E.; Buehner, R. W.; Vandervost, D. Structural and Molecular Characterization of Polyesters by MALDI Mass Spectrometry. 18th Southern Ontario Ion Chemistry Conference, August 13-15, 2001, Leslie Frost Center, Ontario, Canada. Talk: *Arnould, M. A.; Wesdemiotis, C. Characterization of Polybutadienes with Functional End Groups by MALDI Mass Spectrometry. 50th ASMS Conference, June 6-12, 2002, Orlando, FL. Talk: * Wesdemiotis, C; Arnould, M. A.; Gomochak, D.; Quirk, R. P. Effect of Chain-end Functionality on Polymer Composition in Living Anionic Polymerizations. Talk: *Arnould, M. A.; Wesdemiotis, C.; Buehner, R.; Vargas, R. R. Sequence determination of Polyester Copolymers. 224th National ACS Meeting, August 18-22, 2002, Boston, MA. Talk: *Quirk, R. P.; Gomochak, Deanna, L.; Wesdemiotis, Chrys; Arnould, M. A. Synthesis of Diene-Functionalized Macromonomers via Functionalization of Polymeric Organolithiums with 3,4-epoxy-1-butene. 225th National ACS Meeting, March 23-27, 2003, New orleans, LA. Talk: *Wesdemiotis, Chrys; Arnould, M. A.; Quirk, R. P. End Group Characterization in Anionic Polymerizations via Mass Spectrometry Methods. 225th National ACS Meeting, March 23-27, 2003, New orleans, LA. Talk: *Quirk, R. P.; Guo, Ya; Wesdemiotis, Chrys; Arnould, M. A. Functionalization of Polymeric Organolithium Compounds with Formaldehyde. ................................ Of all the things I've lost in life, I miss my mind the most. Mailing AddressDr. Mark A. Arnould, National Institute of Standards and Technology (NIST), 100 Bureau Drive, Polymers Division, Bldg. 224, Rm. B330, Stop 8541, Gaithersburg, MD 20899-8541 |
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NIST Materials Science & Engineering Laboratory - Polymers Division |