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Title SPECTROPHOTOMETRIC DETERMINATION OF TRACES OF BORON IN THORIUM
Creator/Author Onishi, H. ; Ishiwatari, N. ; Nagai, H.
Publication Date1960 Dec 01
OSTI IdentifierOSTI ID: 4073486
Resource TypeJournal Article
Resource RelationBull. Chem. Soc. Japan; Vol: 33
Research OrgJapan Atomic Energy Research Inst., Tokyo
SubjectCHEMISTRY; BORATES; BORON; CURCUMIN; DISTILLATION; METHYL RADICALS; PHOSPHORIC ACID; PHOTOMETRY; QUANTITATIVE ANALYSIS; SEPARATION PROCESSES; SOLUTIONS; SPECTRA; THORIUM; THORIUM OXIDES
Description/Abstract A procedure is described for the spectrophotometric determination of a few tenths of a pant per million of boron ia thorium oxide or thorium. The sample is dissolved in strong phosphoric acid. After diluting the solution with water, boron is separated by distillation as methyl borate and finally determined by the curcumin method. The error is not likely to exceed plus or minus O.l ppm for 0.2 to 1 ppm of boron. (auth)
LanguageEnglish
FormatPages: 1686-8
System Entry Date2001 Jun 03

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