TITLE Field Study Results for VOCs with the Perkin-Elmer Sequential Tube Sampler AUTHOR(S) Maribel Colon and William A. McClenny, Keith G. Kronmiller, Christopher R. Fortune, and E. Hunter Daughtrey, Jr. PERFORMING ORGANIZATION NAME AND ADDRESS National Exposure Research Laboratory Office of Research and Development U.S. Environmental Protection Agency Research Triangle Park, NC 27711 ManTech Environmental Technology, Inc. 2 Triangle Drive Research Triangle Park, NC 27711 SPONSORING AGENCY NAME AND ADDRESS National Exposure Research Laboratory Office of Research and Development U.S. Environmental Protection Agency Research Triangle Park, NC 27711 ABSTRACT Two Perkin-Elmer Sequential Tube Samplers (Model STS-25) were evaluated for their performance, portability, and convenience of operation. Results obtained from both samplers and from a collocated Summa-polished stainless steel canister were compared for seven 3-h periods at three sites. Special attention was given to the monitoring of carbonyl sulfide and carbon disulfide. The samplers were loaded with three sampling tubes, each one packed with 70 mg of Carboxen 1000 (60/80 mesh) and 160 mg of Carbotrap graphitized carbon black (20/40 mesh). An identical tube was used as a field blank. Each tube collected 1200 cm3 of ambient air (20 cm3/min for 60 min). At the end of each sampling period, tubes were sealed and stored in a capped glass tube to prevent contamination and for transportation to a mobile laboratory for analysis. Advantages for the use of the STS-25 are low cost, portability, ease of use, and a design suitable for obtaining sub- part-per-billion detection limits with a standard analytical finish. Disadvantages are that it is a *one-short* technique and no universal solid adsorbent material exists.